Tetraethylammonium tetrachloroferrate (III) C8Cl4FeH20N, S.F.Parker, ISIS Facility C (CM-1) COUNTS ERROR 24.2571,0.299622,0.0292938 24.3784,0.34199,0.031431 24.5003,0.280444,0.0283338 24.6228,0.332552,0.0305151 24.7459,0.36006,0.0320141 24.8696,0.336138,0.0308599 24.994,0.337506,0.0305216 25.119,0.326632,0.030259 25.2446,0.338366,0.0307022 25.3708,0.329302,0.0300173 25.4976,0.341672,0.030525 25.6251,0.357833,0.0312085 25.7533,0.381769,0.0319046 25.882,0.403064,0.0329392 26.0114,0.383677,0.0317526 26.1415,0.390311,0.0320089 26.2722,0.380921,0.0318154 26.4036,0.435502,0.0338123 26.5356,0.37017,0.0309976 26.6682,0.409552,0.0324509 26.8016,0.469967,0.0346193 26.9356,0.43805,0.0334057 27.0703,0.436025,0.0330873 27.2056,0.419906,0.0326928 27.3417,0.459416,0.033875 27.4784,0.473294,0.0343518 27.6158,0.439774,0.0330307 27.7538,0.466651,0.0337132 27.8926,0.459688,0.0336585 28.0321,0.479317,0.0341233 28.1722,0.446322,0.0328073 28.3131,0.456391,0.0331706 28.4547,0.440742,0.0323385 28.5969,0.530395,0.035427 28.7399,0.551554,0.0358558 28.8836,0.48468,0.0335831 29.028,0.511431,0.0343768 29.1732,0.431721,0.0312878 29.319,0.493491,0.0332847 29.4656,0.60232,0.0367597 29.613,0.530787,0.0344808 29.761,0.572646,0.035948 29.9098,0.481096,0.0326969 30.0594,0.511126,0.0333743 30.2097,0.532881,0.0340892 30.3607,0.564754,0.0350098 30.5125,0.584491,0.0354964 30.6651,0.5612,0.0347007 30.8184,0.58634,0.0354405 30.9725,0.598904,0.0357677 31.1274,0.60445,0.0357063 31.283,0.615008,0.0361018 31.4394,0.648309,0.0365786 31.5966,0.570542,0.0342641 31.7546,0.524675,0.0328987 31.9134,0.596287,0.0348677 32.0729,0.548217,0.0332888 32.2333,0.560424,0.0337525 32.3945,0.524455,0.0324044 32.5564,0.558939,0.0332317 32.7192,0.541146,0.0327382 32.8828,0.489893,0.0310508 33.0472,0.602912,0.0343516 33.2125,0.552863,0.0327223 33.3785,0.550864,0.0326528 33.5454,0.518136,0.0313957 33.7132,0.553656,0.0324966 33.8817,0.578183,0.0332554 34.0511,0.581634,0.0329304 34.2214,0.51651,0.0309691 34.3925,0.462855,0.0293065 34.5645,0.545962,0.0316283 34.7373,0.595338,0.0330004 34.911,0.541055,0.0314403 35.0855,0.537217,0.0311222 35.2609,0.553714,0.0314035 35.4373,0.51684,0.0303047 35.6144,0.57218,0.0317522 35.7925,0.496824,0.0296694 35.9715,0.544283,0.0308826 36.1513,0.508382,0.029734 36.3321,0.489246,0.0291354 36.5137,0.493581,0.0292643 36.6963,0.466783,0.0282411 36.8798,0.532756,0.0300448 37.0642,0.469865,0.0282325 37.2495,0.465652,0.0280036 37.4358,0.469543,0.027917 37.6229,0.449495,0.0272608 37.8111,0.428723,0.0264323 38.0001,0.424606,0.0262755 38.1901,0.397536,0.0254316 38.3811,0.457178,0.0269653 38.573,0.45322,0.0268973 38.7658,0.471639,0.0273658 38.9597,0.395999,0.0250188 39.1545,0.405386,0.0252666 39.3502,0.404497,0.0250597 39.547,0.390391,0.0244531 39.7447,0.419871,0.0254308 39.9434,0.437438,0.0258624 40.1432,0.419459,0.0252414 40.3439,0.399694,0.0245254 40.5456,0.45986,0.0261179 40.7483,0.394117,0.0241259 40.9521,0.417331,0.0249319 41.1568,0.426937,0.0251321 41.3626,0.416025,0.0246623 41.5694,0.448291,0.0255275 41.7773,0.436417,0.02504 41.9862,0.419375,0.0245154 42.1961,0.499108,0.0266398 42.4071,0.480354,0.026112 42.6191,0.474806,0.0258386 42.8322,0.472923,0.0257518 43.0464,0.457225,0.025375 43.2616,0.459062,0.02528 43.4779,0.461063,0.02529 43.6953,0.47001,0.025472 43.9138,0.420531,0.0239383 44.1333,0.387588,0.0229547 44.354,0.429382,0.0240549 44.5758,0.381849,0.0226591 44.7987,0.367555,0.0221472 45.0226,0.358044,0.0218215 45.2478,0.312815,0.0203077 45.474,0.339098,0.0211414 45.7014,0.307663,0.020108 45.9299,0.276573,0.0189817 46.1595,0.22398,0.0170291 46.3903,0.204581,0.0161522 46.6223,0.171692,0.0148135 46.8554,0.151178,0.0138273 47.0897,0.179674,0.0148227 47.3251,0.165394,0.0141203 47.5617,0.213025,0.0160189 47.7995,0.261603,0.0176416 48.0385,0.319618,0.0193744 48.2787,0.376673,0.021044 48.5201,0.460068,0.0233111 48.7627,0.516126,0.0246439 49.0065,0.589603,0.0263091 49.2516,0.695515,0.0285076 49.4978,0.770991,0.0300076 49.7453,0.772889,0.029965 49.994,0.729399,0.029027 50.244,0.766243,0.0297158 50.4952,0.787863,0.0300146 50.7477,0.751701,0.0293256 51.0015,0.760211,0.0293754 51.2565,0.725961,0.0286302 51.5127,0.711629,0.0282915 51.7703,0.724591,0.028423 52.0292,0.712462,0.0280805 52.2893,0.652093,0.0268071 52.5507,0.708815,0.0278797 52.8135,0.701115,0.0276708 53.0776,0.704566,0.027664 53.343,0.746333,0.0283786 53.6097,0.681567,0.0270772 53.8777,0.678971,0.026916 54.1471,0.648148,0.0262578 54.4178,0.640516,0.0259721 54.6899,0.5687,0.02439 54.9634,0.563739,0.0241114 55.2382,0.537261,0.0234872 55.5144,0.519438,0.0230406 55.792,0.588273,0.0244909 56.0709,0.648062,0.0257023 56.3513,0.657413,0.0257693 56.633,0.709844,0.0266746 56.9162,0.744395,0.0273174 57.2008,0.69131,0.0262251 57.4868,0.669162,0.025765 57.7742,0.727212,0.0267429 58.0631,0.747022,0.0270498 58.3534,0.739717,0.0268398 58.6452,0.738695,0.0267129 58.9384,0.717508,0.0262456 59.2331,0.750668,0.0267808 59.5293,0.697376,0.0257246 59.8269,0.735273,0.0262859 60.126,0.741195,0.0263494 60.4267,0.682847,0.0251703 60.7288,0.725241,0.0257955 61.0324,0.765224,0.0263769 61.3376,0.85611,0.0278774 61.6443,0.986209,0.0297951 61.9525,0.951721,0.0292374 62.2623,0.984175,0.029636 62.5736,1.00553,0.0298845 62.8865,1.04794,0.030457 63.2009,1.04948,0.0304066 63.5169,1.03607,0.0301212 63.8345,1.00606,0.0295927 64.1537,0.93638,0.0285273 64.4744,0.884759,0.0276472 64.7968,0.811333,0.0263883 65.1208,0.780351,0.0257904 65.4464,0.721696,0.0246593 65.7736,0.735722,0.0247923 66.1025,0.787056,0.0254965 66.433,0.839808,0.0262464 66.7652,0.923676,0.0274786 67.099,1.01504,0.0287182 67.4345,1.10034,0.0298189 67.7716,1.1808,0.0308849 68.1105,1.23794,0.0314974 68.4511,1.2989,0.032209 68.7933,1.33833,0.0326257 69.1373,1.2666,0.0316188 69.483,1.2625,0.0315158 69.8304,1.23464,0.0311397 70.1795,1.21468,0.0307767 70.5304,1.16844,0.030052 70.8831,1.06342,0.0285728 71.2375,1.11554,0.0291617 71.5937,1.1198,0.0291124 71.9517,1.02904,0.0278025 72.3114,1.13575,0.0291026 72.673,1.22543,0.0301978 73.0363,1.19636,0.0297568 73.4015,1.22977,0.0301003 73.7685,1.2574,0.0303845 74.1374,1.1543,0.029038 74.5081,1.20765,0.0296458 74.8806,1.13414,0.0285902 75.255,1.11078,0.0281859 75.6313,1.10308,0.0279559 76.0094,1.12795,0.0282826 76.3895,1.15056,0.0284223 76.7714,1.12383,0.0280647 77.1553,1.18351,0.0287122 77.5411,1.1194,0.0278737 77.9288,1.01963,0.0265542 78.3184,0.99968,0.0262272 78.71,0.880309,0.0245438 79.1035,0.843061,0.0239184 79.4991,0.853712,0.0240233 79.8966,0.823473,0.0235505 80.296,0.779066,0.0227976 80.6975,0.86262,0.0239276 81.101,0.883977,0.0241459 81.5065,0.955098,0.0250143 81.9141,0.944762,0.0247966 82.3236,1.06951,0.0262963 82.7352,1.19092,0.0276653 83.1489,1.34026,0.0292966 83.5647,1.47048,0.0306229 83.9825,1.6817,0.0327284 84.4024,1.68273,0.0326975 84.8244,1.73138,0.0330996 85.2485,1.78993,0.0336118 85.6748,1.77948,0.0333956 86.1031,1.64041,0.0320089 86.5337,1.63489,0.0318875 86.9663,1.50948,0.0305637 87.4012,1.49582,0.0303196 87.8382,1.49932,0.0302317 88.2774,1.62171,0.0314234 88.7187,1.66663,0.0317429 89.1623,1.6222,0.0312288 89.6082,1.6425,0.0312888 90.0562,1.6792,0.0315598 90.5065,1.63941,0.0311119 90.959,1.60622,0.0307254 91.4138,1.53232,0.0298725 91.8709,1.4703,0.0292079 92.3302,1.3624,0.0280196 92.7919,1.29566,0.0272464 93.2558,1.21158,0.0262986 93.7221,1.1295,0.0252907 94.1907,1.03826,0.0241999 94.6617,0.958048,0.0231836 95.135,0.843485,0.0216668 95.6107,0.761365,0.0204742 96.0887,0.781045,0.0206609 96.5692,0.825979,0.0211299 97.052,0.959644,0.0226451 97.5373,1.22286,0.0254505 98.0249,1.59651,0.0290365 98.5151,2.00264,0.032517 99.0076,2.42824,0.0357966 99.5027,2.6869,0.0376725 100,2.56528,0.0367914 100.5,2.23076,0.0342495 101.003,1.76115,0.0304104 101.508,1.17903,0.0248114 102.015,0.747092,0.0196508 102.525,0.4959,0.0159237 103.038,0.385079,0.0139922 103.553,0.304173,0.0124151 104.071,0.265149,0.0115549 104.591,0.248028,0.0111137 105.114,0.212528,0.0102901 105.64,0.217542,0.010389 106.168,0.197481,0.00987269 106.699,0.21864,0.0103439 107.232,0.198628,0.00983871 107.768,0.181248,0.00939359 108.307,0.186472,0.00951246 108.849,0.19615,0.00972807 109.393,0.177772,0.00927858 109.94,0.193071,0.00961599 110.49,0.198056,0.00972008 111.042,0.215674,0.0100809 111.597,0.207905,0.00984116 112.155,0.213896,0.00998598 112.716,0.239017,0.0105002 113.28,0.267793,0.0110976 113.846,0.29866,0.0116479 114.415,0.398196,0.0133792 114.987,0.486194,0.0147479 115.562,0.661673,0.017131 116.14,0.891942,0.0198623 116.721,1.18159,0.0228457 117.305,1.51793,0.0258715 117.891,1.79448,0.0280849 118.481,1.8587,0.0285147 119.073,1.89036,0.0287044 119.668,1.95808,0.0291065 120.267,2.07758,0.0299245 120.868,2.16247,0.0304943 121.472,2.09496,0.0299865 122.08,1.87266,0.0282673 122.69,1.66412,0.0265614 123.304,1.59714,0.0259217 123.92,1.67902,0.0264699 124.54,1.76372,0.0270603 125.162,1.85875,0.0277627 125.788,1.82743,0.027459 126.417,1.6268,0.0258938 127.049,1.31944,0.0233002 127.684,0.986546,0.0201003 128.323,0.679435,0.0166428 128.964,0.457493,0.013605 129.609,0.35023,0.0118547 130.257,0.310871,0.0111245 130.909,0.289089,0.0106969 131.563,0.276912,0.0104416 132.221,0.280897,0.0104753 132.882,0.305839,0.0108893 133.546,0.323258,0.0111579 134.214,0.400206,0.0123803 134.885,0.445228,0.0130382 135.56,0.514141,0.0139916 136.238,0.615013,0.0152643 136.919,0.663135,0.0158047 137.603,0.682488,0.0159992 138.291,0.729661,0.016533 138.983,0.785163,0.0171289 139.678,0.698976,0.0160978 140.376,0.62532,0.0151935 141.078,0.567043,0.0144504 141.783,0.48795,0.0133685 142.492,0.456426,0.0128855 143.205,0.422114,0.0123521 143.921,0.46438,0.01291 144.64,0.491359,0.0132178 145.364,0.592854,0.0144743 146.09,0.765592,0.0163844 146.821,1.08463,0.0194519 147.555,1.50849,0.0228823 148.293,1.97109,0.0261369 149.034,2.3521,0.0285379 149.779,2.43678,0.0290409 150.528,2.14058,0.0271603 151.281,1.70639,0.0242 152.037,1.21364,0.0203544 152.797,0.886682,0.0173511 153.561,0.653651,0.0148666 154.329,0.509577,0.013098 155.101,0.44123,0.0121555 155.876,0.413697,0.0117336 156.656,0.384278,0.0112647 157.439,0.357386,0.0108392 158.226,0.350758,0.0107356 159.017,0.358262,0.0107944 159.812,0.335811,0.0104283 160.612,0.322313,0.0101939 161.415,0.335984,0.0103704 162.222,0.371608,0.0108937 163.033,0.38541,0.0110635 163.848,0.409919,0.0114046 164.667,0.465999,0.0120982 165.491,0.590565,0.0135635 166.318,0.787971,0.0156398 167.15,1.11307,0.0185701 167.985,1.45655,0.0212222 168.825,1.68797,0.0228591 169.669,1.65314,0.0225981 170.518,1.42104,0.0209378 171.37,1.04714,0.0179489 172.227,0.741155,0.015057 173.088,0.570486,0.0131997 173.954,0.456861,0.0117773 174.823,0.400919,0.011007 175.698,0.35257,0.0103012 176.576,0.330062,0.00994449 177.459,0.306878,0.00956395 178.346,0.294761,0.00935409 179.238,0.295631,0.00935652 180.134,0.274785,0.00900273 181.035,0.269584,0.00890524 181.94,0.265261,0.00878937 182.85,0.267684,0.00882483 183.764,0.270254,0.00884366 184.683,0.280289,0.00898349 185.606,0.263237,0.00868175 186.534,0.274067,0.00883993 187.467,0.274147,0.00881179 188.404,0.282589,0.00894017 189.346,0.278366,0.00885176 190.293,0.274009,0.00876325 191.244,0.28124,0.00886951 192.201,0.265979,0.00859217 193.162,0.26025,0.00848655 194.128,0.247048,0.00823741 195.098,0.252955,0.00831335 196.074,0.250889,0.00826413 197.054,0.259309,0.00840187 198.039,0.270849,0.00856579 199.029,0.289713,0.00884306 200.025,0.319382,0.0092653 201.025,0.323193,0.00929934 202.03,0.315977,0.00917131 203.04,0.314782,0.00913847 204.055,0.307793,0.00901539 205.075,0.323763,0.00921503 206.101,0.33793,0.0094154 207.131,0.365889,0.00975137 208.167,0.403609,0.0102269 209.208,0.526105,0.0116479 210.254,0.666433,0.0130778 211.305,0.879317,0.0149962 212.362,1.11901,0.0168871 213.424,1.26755,0.01798 214.491,1.24038,0.0177664 215.563,0.988593,0.0158295 216.641,0.717328,0.0134541 217.724,0.529795,0.0115445 218.813,0.447172,0.0105959 219.907,0.384907,0.0097989 221.006,0.373553,0.00963687 222.111,0.326183,0.00899785 223.222,0.323109,0.00893014 224.338,0.310882,0.00874432 225.46,0.300771,0.00859832 226.587,0.289253,0.00840245 227.72,0.277752,0.00822935 228.859,0.273583,0.00815051 230.003,0.310921,0.00866166 231.153,0.37156,0.00945197 232.309,0.438855,0.0102484 233.47,0.592438,0.0118694 234.638,0.84459,0.0141408 235.811,1.23508,0.0170676 236.99,1.61395,0.0194775 238.175,1.8054,0.020578 239.366,1.77667,0.0204118 240.562,1.65749,0.0196819 241.765,1.42081,0.0182009 242.974,1.109,0.016044 244.189,0.863163,0.014133 245.41,0.770347,0.0133197 246.637,0.772387,0.0133229 247.87,0.907139,0.0144107 249.109,1.10045,0.0158507 250.355,1.38267,0.0177358 251.607,1.75745,0.0199646 252.865,2.0899,0.0217337 254.129,2.10784,0.0218078 255.4,1.69984,0.0195791 256.677,1.15102,0.0160667 257.96,0.900356,0.014171 259.25,0.9534,0.0145571 260.546,1.20442,0.0163248 261.849,1.48703,0.0181191 263.158,1.59685,0.0187586 264.474,1.35682,0.0172837 265.796,0.906045,0.0141017 267.125,0.645611,0.0118845 268.461,0.540021,0.0108371 269.803,0.534207,0.0107718 271.152,0.526585,0.0106638 272.508,0.611949,0.0114711 273.871,0.721278,0.012434 275.24,0.994342,0.014581 276.616,1.35666,0.0170087 277.999,1.57133,0.0182952 279.389,1.46355,0.0176393 280.786,1.06706,0.0150477 282.19,0.659553,0.0118086 283.601,0.426546,0.00948315 285.019,0.370695,0.00882645 286.444,0.361139,0.00870303 287.876,0.370348,0.00879492 289.316,0.383469,0.0089441 290.762,0.379685,0.00888341 292.216,0.381683,0.00890756 293.677,0.388283,0.0089705 295.146,0.394196,0.00901672 296.621,0.391291,0.00897044 298.104,0.398622,0.00904154 299.595,0.381374,0.00883743 301.093,0.352764,0.00849097 302.598,0.346032,0.00838869 304.111,0.353736,0.00848422 305.632,0.346681,0.00839173 307.16,0.345752,0.00836456 308.696,0.352953,0.00844072 310.239,0.353137,0.00843879 311.791,0.371477,0.00863076 313.35,0.402355,0.00896946 314.916,0.430874,0.00927677 316.491,0.465503,0.00962461 318.073,0.540854,0.0103762 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